Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,6-Di-tert-butyl-4-mercaptophenol → 1,4-Bis[2-(3,5-di-tert-butyl-4-hydroxyphenylthio)succinimido]-benzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,6-Di-tert-butyl-4-mercaptophenol | HCID 70370 | — |
| 반응물 | 1,4-Phenylenebismaleimide | HCID 76765 | — |
| 용매 | Triethylamine | HCID 8471 | — |
| 생성물 | 1,4-Bis[2-(3,5-di-tert-butyl-4-hydroxyphenylthio)succinimido]-benzene | HCID 13547666 | 75.6% |
반응 단계
The procedure of Example 1 is repeated using 17.8 grams of 2,6-di-tert-butyl-4-mercaptophenol, 10 grams of 1,4-bis(maleimido)benzene, and 0.75 grams of triethylamine. The residue is recrystallized from acetone to give 21 grams of an off-white solid, m.p. 274°-278° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04456716 |
| 출처 데이터셋 | uspto-grants-1984_06 |
| ORD ID | ord-b2ff3ff2a03c4dddbb8002f06af91f29 |
| 출처 메모 | uspto-grants-1984_06 |