Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5-Methoxyisatin → HCID 178487247, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5-Methoxyisatin | HCID 38333 | — |
| 반응물 | 4-Hydrazinylbenzenesulfonamide hydrochloride | HCID 2794567 | — |
| 생성물 | HCID 178487247 | HCID 178487247 | — |
반응 단계
The title compound was prepared from 5-methoxy-1H-indole-2,3-dione (Gassman, et al., Journal of Organic Chemistry 1977, 42, 1344-8) and 4-hydrazinobenzenesulfonamide hydrochloride according to Procedure G: mp>250° C.; 1H NMR (DMSO-d6): δ 3.80 (s, 3H), 6.87 (s, 2H), 7.20 (s, 1H), 7.28 (s, 2H), 7.60 (d, J=8.8 Hz, 2H), 7.81 (d, J=8.8 Hz, 2H), 10.93 (s, 1H), 12.85 (s, 1H); APCI−MS m/z 344.9 (M−H)−.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06541503B2 |
| 출처 데이터셋 | uspto-grants-2003_04 |
| ORD ID | ord-6024488a854b4596b3ebe20391d847a0 |
| 출처 메모 | uspto-grants-2003_04 |