Hydrazine → 1-Cyclohexyl-1-phenyl-hydrazine

HRID 127960

반응식

[CH:1]1([N:7]([N:14]=O)[C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.C1(NC2C=CC=CC=2)CCCCC1.NN.[H-].[Al+3].[Li+].[H-].[H-].[H-]>>[CH:8]1([N:7]([C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)[NH2:14])[CH2:9][CH2:10][CH2:11][CH2:12][CH2:13]1

참가 물질

반응물 4

HCID 9321Hydrazine

HCID 74567N-Cyclohexylaniline

HCID 21226445Aluminium lithium hydride

HCID 23471014N-Cyclohexyl-N-phenylnitrous amide

생성물 1

HCID 128663281-Cyclohexyl-1-phenyl-hydrazine

실험 절차

N-Cyclohexyl-N-nitrosoaniline, prepared from N-cyclohexylaniline by the method described in Example 1 was subsequently reduced to the hydrazine by the lithium aluminum hydride method described in Example 4. 1-Cyclohexyl-1-phenyl hydrazine distilled at 120°-150° C./0.2 mm.

후처리

distillation1-Cyclohexyl-1-phenyl hydrazine distilled at 120°-150° C./0.2 mm

출처 및 근거

ORD 기록: ord-1359a50870784657a2321d5ed8fa712e
출처 데이터셋: uspto-grants-1981_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04258059

연결된 노트

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