Hydroxide → 1-Phenyl-2-propanol
반응식
O.[OH-].[C:3]1([CH2:9][C:10](=[O:12])[CH3:11])[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1>C(O)C>[C:3]1([CH2:9][CH:10]([OH:12])[CH3:11])[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1참가 물질
5
반응 조건
- 온도
- 80 °C
실험 절차
In a 4 liter three-necked flask fitted with a mechanical stirrer and a reflux condenser, were placed 1500 ml of water, 150 g ofsodium hydroxide (pellets), 190 ml of ethanol and 180 g of phenylacetone. The mixture was stirred and heated to 80° C., and 150 g of Raney alloy was added very cautiously by small amounts over about 1 hour. During the addition, heating was discontinued and the temperature was maintained at 85°-87° C.
후처리
- customIn a 4 liter three-necked flask fitted with a mechanical stirrer and a reflux condenser
- addition150 g of Raney alloy was added very cautiously by small amounts over about 1 hour
- additionDuring the addition
- temperatureheating
- temperaturethe temperature was maintained at 85°-87° C.
출처 및 근거
- ORD 기록
- ord-6fb44f952434407bb6a64e1190cd6c08
- 출처 데이터셋
- uspto-grants-1981_03
- 특허 번호
- US04258120
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