Hydrochloric Acid → Benzenediazonium, 4-methoxy-, chloride

HRID 128002노트

반응식

HRID 128002 반응식
[N:1]([O-])=O.[Na+].[CH3:5][O:6][C:7]1[CH:12]=[CH:11][C:10]([NH2:13])=[CH:9][CH:8]=1.[ClH:14]>O>[Cl-:14].[CH3:5][O:6][C:7]1[CH:12]=[CH:11][C:10]([N+:13]#[N:1])=[CH:9][CH:8]=1

참가 물질

5

반응물 3

HCID 313Hydrochloric AcidHCID 7732P-AnisidineHCID 23668193Sodium Nitrite

생성물 1

HCID 11829892Benzenediazonium, 4-methoxy-, chloride수율 77%

시약·촉매·용매 1

HCID 962Water용매2회

실험 절차

A solution of 4-methoxy-phenyl-diazonium chloride was prepared by adding dropwise at 0° C. a solution of 1.8 g of sodium nitrite dissolved in 2.5 ml of water to a solution of 3.075 g of p-anisidine dissolved in 25 ml of water and 8.1 ml of concentrated hydrochloric acid. The reaction mixture was allowed to stand for 2 hours.

출처 및 근거

ORD 기록
ord-3bf2fabb883b43b583957c7643dfea67
출처 데이터셋
uspto-grants-1981_03
특허 번호
US04258120

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