Methanol → 2-Methoxycarbonyl-6-methyl-benzo[b] thiophene-3-sulfonic acid chloride

HRID 128282노트

반응식

HRID 128282 반응식
Cl[C:2]([C:4]1[S:8][C:7]2[CH:9]=[C:10]([CH3:13])[CH:11]=[CH:12][C:6]=2[C:5]=1[S:14]([Cl:17])(=[O:16])=[O:15])=[O:3].[CH3:18][OH:19]>C(Cl)(Cl)Cl>[CH3:18][O:19][C:2]([C:4]1[S:8][C:7]2[CH:9]=[C:10]([CH3:13])[CH:11]=[CH:12][C:6]=2[C:5]=1[S:14]([Cl:17])(=[O:15])=[O:16])=[O:3]

참가 물질

4

반응물 2

HCID 887MethanolHCID 538745162-Chlorocarbonyl-6-methyl-benzo[b] thiophene-3-sulfonic acid chloride

생성물 1

HCID 544583022-Methoxycarbonyl-6-methyl-benzo[b] thiophene-3-sulfonic acid chloride

시약·촉매·용매 1

HCID 6212Chloroform용매

실험 절차

Prepared analogous to Example 1(c) from 2-chlorocarbonyl-6-methyl-benzo[b] thiophene-3-sulfonic acid chloride and methanol in the presence of chloroform.

출처 및 근거

ORD 기록
ord-b360b6b8f62e4cf2abdaaa69480bc38f
출처 데이터셋
uspto-grants-1981_03
특허 번호
US04259336

반응 노트

불러오는 중…