Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Carbonate → HCID 54335838, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | Hexamethylphosphoramide | HCID 12679 | — |
| 반응물 | Ethyl 3-(4-aminophenyl)acrylate | HCID 97826 | — |
| 반응물 | (4-Bromobutyl)cycloheptane | HCID 13131543 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | HCID 54335838 | HCID 54335838 | — |
반응 단계
A mixture of ethyl p-aminocinnamate, 5.9 g. 4-bromobutylcycloheptane and one equivalent of anhydrous powdered potassium carbonate in 50 ml. hexamethylphosphoramide is heated for 20 hours at 60° C. The mixture is then cooled, diluted with water and extracted with ether. The combined ether extracts are dried, filtered and evaporated. Crystallization from acetonitrile provides the title compound as white crystals.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04259352 |
| 출처 데이터셋 | uspto-grants-1981_03 |
| ORD ID | ord-066ba254822146d2a4d93aa6ba85e614 |
| 출처 메모 | uspto-grants-1981_03 |