HCID 178479391, 화합물 → HCID 178512583, 화합물

HRID 1283742노트

반응식

HRID 1283742 반응식
Cl.[Cl:2][C:3]1[CH:8]=[CH:7][CH:6]=[C:5]([Cl:9])[C:4]=1[NH:10][C:11]([NH2:13])=[NH:12]>[OH-].[Na+]>[Cl:2][C:3]1[CH:8]=[CH:7][CH:6]=[C:5]([Cl:9])[C:4]=1[NH:10][C:11]([NH2:13])=[NH:12]

참가 물질

3

반응물 1

HCID 178479391HCID 178479391, 화합물

생성물 1

HCID 178512583HCID 178512583, 화합물

시약·촉매·용매 1

HCID 14798Sodium Hydroxide용매

실험 절차

The free base is prepared by dissolving 2,6-dichlorophenylguanidine hydrochloride in 10% sodium hydroxide solution and extracting with ether. The ether is dried and evaporated to dryness to obtain 2,6-dichlorophenylguanidine.

후처리

  1. customThe free base is prepared
  2. extractionextracting with ether
  3. dry with materialThe ether is dried
  4. customevaporated to dryness

출처 및 근거

ORD 기록
ord-50798862fe09478da5be7d7a40642343
출처 데이터셋
uspto-grants-1976_08
특허 번호
US03976643

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