1,4-Bis(3-aminopropyl)piperazine → (3-Chloropropanoyl)urea

HRID 1283996

반응식

HRID 1283996 반응식
[NH2:1]CCCN1CCN(CCCN)CC1.[Cl:15][CH2:16][CH2:17][C:18]([N:20]=[C:21]=[O:22])=[O:19]>>[Cl:15][CH2:16][CH2:17][C:18]([NH:20][C:21]([NH2:1])=[O:22])=[O:19]

참가 물질

3

반응물 2

HCID 816291,4-Bis(3-aminopropyl)piperazineHCID 135723743-Chloropropanoyl isocyanate

생성물 1

HCID 12937417(3-Chloropropanoyl)urea수율 318.8%

실험 절차

In the same way as in Example 1, reaction of 10.0 g (50 mmols) of N,N'-bis(3-aminopropyl)piperazine with 14.3 g (106 mmols) of 3-chloropropionyl isocyanate gives 24.0 g of the 3-chloropropionylurea compound of the formula ##STR10##

출처 및 근거

ORD 기록
ord-82fa546ce33a4994a61a30075cc98ded
출처 데이터셋
uspto-grants-1976_08
특허 번호
US03977881

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