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llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
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Acetonitrile → Pentanenitrile, 4,4-dimethyl-3-oxo-

HRID 128431
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HRID 128431 반응식
[H-].[Na+].[C:3]([O:9]C)(=O)[C:4]([CH3:7])([CH3:6])[CH3:5].[C:11](#[N:13])[CH3:12]>O1CCCC1>[C:3]([CH2:12][C:11]#[N:13])(=[O:9])[C:4]([CH3:7])([CH3:6])[CH3:5]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

5

반응물 3

HCID 6342AcetonitrileHCID 24758Sodium hydrideHCID 69027Methyl pivalate

생성물 1

HCID 108871Pentanenitrile, 4,4-dimethyl-3-oxo-

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매2회

실험 절차

In a 1 l. flask under an atmosphere of dry nitrogen there was placed 26.4 g. of a 50% oil dispersion of sodium hydride together with 240 ml. of dry tetrahydrofuran. While this mixture was refluxed there was added thereto dropwise over a period of about 1 hour a mixture of 40.6 g. of methyl pivalate and 22.6 g. of acetonitrile in 40 ml. of dry tetrahydrofuran. When addition was complete, the mixture was refluxed overnight. The reaction mixture was worked up by evaporating part of the tetrahydrofuran in vacuo and dissolving the remaining solution in about 300 ml. of water. This aqueous mixture was acidified to about pH 4 using concentrated aqueous hydrochloric acid. The remainder of the tetrahydrofuran was then removed using a rotovapor. The solid which was formed was filtered and slurried with 150 ml. of hexane to remove mineral oil. The crystals were filtered and dried. The crystals had a melting point of about 57°-59° C. and were identified as pivalyl acetonitrile. Yield: 36.3 g. (83%).

후처리

  1. customflask under an atmosphere of dry nitrogen there was placed
  2. temperatureWhile this mixture was refluxed there
  3. additionwas added
  4. additiondropwise over a period of about 1 hour a mixture of 40.6 g
  5. additionWhen addition
  6. temperaturethe mixture was refluxed overnight
  7. customby evaporating part of the tetrahydrofuran in vacuo
  8. dissolutiondissolving the remaining solution in about 300 ml
  9. customThe remainder of the tetrahydrofuran was then removed
  10. customThe solid which was formed
  11. filtrationwas filtered
  12. customof hexane to remove mineral oil
  13. filtrationThe crystals were filtered
  14. customdried

출처 및 근거

ORD 기록
ord-355fc2bf84d64590b798bae7814bd719
출처 데이터셋
uspto-grants-1981_03
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04259501

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