Water → HCID 6404487, 화합물

HRID 1285122노트

반응식

HRID 1285122 반응식
[C:1]1([C:7]2[CH:8]=[C:9]([C:14]([NH2:16])=O)[C:10](=O)[NH:11][N:12]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.O.P(Cl)(Cl)([Cl:20])=O>>[Cl:20][C:10]1[N:11]=[N:12][C:7]([C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)=[CH:8][C:9]=1[C:14]#[N:16]

참가 물질

4

반응물 3

HCID 962WaterHCID 24813Phosphorus oxychlorideHCID 14753284D-083

생성물 1

HCID 6404487HCID 6404487, 화합물

반응 조건

온도
80 °C

실험 절차

1.5 g of the product obtained in Example 1 are dissolved in 20 ml of phosphorus oxychloride and the solution is then heated at 80° C. for 5 hours. The mixture is poured into 50 ml of water. A precipitate appears, which is filtered off and dried.

후처리

  1. filtrationwhich is filtered off
  2. customdried

출처 및 근거

ORD 기록
ord-49d408cfb7874a49b5f9627ff0f2af9a
출처 데이터셋
uspto-grants-1986_01
특허 번호
US04565814

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