Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(1,1'-Biphenyl)-4-sulphonyl chloride → N-(4-Tridecyl-3-trifluoromethyl-5-isoxazolyl)-4-biphenylsulfonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (1,1'-Biphenyl)-4-sulphonyl chloride | HCID 74192 | — |
| 반응물 | 5-Amino-4-tridecyl-3-trifluoromethyl-isoxazole | HCID 15453191 | — |
| 생성물 | N-(4-Tridecyl-3-trifluoromethyl-5-isoxazolyl)-4-biphenylsulfonamide | HCID 15453192 | 81% |
반응 단계
N-(4-Tridecyl-3-trifluoromethyl-5-isoxazolyl)-4-biphenylsulfonamide was prepared, in the same manner as described in Example 2b, from 5-amino-4-tridecyl-3-trifluoromethyl-isoxazole and 4-biphenylsulfonyl chloride in 81% yield. Purification was achieved by recrystallization from methanol/water to give an off white solid, m.p. 115°-116° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05464853 |
| 출처 데이터셋 | uspto-grants-1995_11 |
| ORD ID | ord-58e39f9627cb4cddba8390d650a1854b |
| 출처 메모 | uspto-grants-1995_11 |