Hydrochloric Acid → HCID 21509169, 화합물

HRID 1287509노트

반응식

HRID 1287509 반응식
[ClH:1].[NH2:2][C:3]1[N:4]([CH3:21])[C:5]2[C:10]([C:11]=1[C:12]1[CH:17]=[CH:16][C:15]([N+:18]([O-])=O)=[CH:14][CH:13]=1)=[CH:9][CH:8]=[CH:7][CH:6]=2>[Pd].C(O)C>[ClH:1].[NH2:2][C:3]1[N:4]([CH3:21])[C:5]2[C:10]([C:11]=1[C:12]1[CH:17]=[CH:16][C:15]([NH2:18])=[CH:14][CH:13]=1)=[CH:9][CH:8]=[CH:7][CH:6]=2

참가 물질

5

반응물 2

HCID 313Hydrochloric AcidHCID 134869191-Methyl-3-(4-nitrophenyl)-1H-indol-2-amine

생성물 1

HCID 21509169HCID 21509169, 화합물수율 53%

시약·촉매·용매 2

HCID 23938Palladium촉매HCID 702Ethanol용매

실험 절차

The compound is obtained by hydrogenating at room temperature and atmospheric pressure in the presence 10% Pd on charcoal an ethanol solution of the hydrochloride of 2-amino-1-methyl-3-(p-nitrophenyl) indole. Yield 53%, m.p. 258°-261° C.

후처리

  1. customThe compound is obtained
  2. customby hydrogenating at room temperature

출처 및 근거

ORD 기록
ord-1eb83efcc27345f381510b9992d14e6c
출처 데이터셋
uspto-grants-1976_10
특허 번호
US03984563

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