Hydrochloric Acid → HCID 21503398, 화합물

반응식

C(OC([N:6]1[CH2:20][CH2:19][C:18]2[C:9](=[N:10][C:11]3[CH:12]=[CH:13][CH:14]=[CH:15][C:16]=3[C:17]=2[O:21][CH3:22])[CH2:8][CH2:7]1)=O)C.Cl>>[CH3:22][O:21][C:17]1[C:16]2[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=2[N:10]=[C:9]2[CH2:8][CH2:7][NH:6][CH2:20][CH2:19][C:18]=12

참가 물질

반응물 2

HCID 313Hydrochloric Acid

HCID 5380140911-Methoxy-1,2,4,5-tetrahydro-3-azepino[4,5-b]quinoline-carboxylic acid ethyl ester

생성물 1

HCID 21503398HCID 21503398, 화합물수율 7%

실험 절차

11-methoxy-1,2,4,5-tetrahydro-3H-azepino[4,5-b]quinoline was prepared from 11-methoxy-1,2,4,5-tetrahydro-3-azepino[4,5-b] quinoline-carboxylic acid ethyl ester by hydrolysis with semiconcentrated hydrochloric acid. Yield: 7% of theory; m.p. 112° C.

출처 및 근거

ORD 기록: ord-9972402c51914d2f8bf48c32680d999e
출처 데이터셋: uspto-grants-1976_10
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US03987047

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