Benzene → Phenylthionophosphonic dichloride

HRID 1288486

반응식

HRID 1288486 반응식
[P:1]([Cl:5])(Cl)([Cl:3])=[S:2].[CH:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1>>[C:6]1([P:1]([Cl:5])([Cl:3])=[S:2])[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1

참가 물질

3

반응물 2

HCID 241BenzeneHCID 19883Thiophosphoryl chloride

생성물 1

HCID 19016Phenylthionophosphonic dichloride

반응 조건

온도
200 °C

실험 절차

In a 100 cc autoclave, 42.35 g (0.25 mole) of thiophosphoryl trichloride, 19.53 g (0.25 mole) of benzene were charged, and the mixture was heated with stirring at 200° C for 4 hours. The reaction mixture was treated in accordance with the process of Example 1. No phenylphosphonothioic dichloride was produced.

후처리

  1. temperaturethe mixture was heated
  2. additionThe reaction mixture was treated in accordance with the process of Example 1

출처 및 근거

ORD 기록
ord-3415756249a948d698066d8c2ad191f4
출처 데이터셋
uspto-grants-1976_10
특허 번호
US03988368

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