Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
[1-Methyl-3-(2,6,6-trimethyl-2-cyclohexenyl)-2(trans)-propenyl]dimethyl(4-chlorobenzyl)ammonium iodide → [1-Methyl-3-(2,6,6-trimethyl-2-cyclohexenyl)-2(trans)-propenyl]dimethyl(4-chlorobenzyl)ammonium chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | [1-Methyl-3-(2,6,6-trimethyl-2-cyclohexenyl)-2(trans)-propenyl]dimethyl(4-chlorobenzyl)ammonium iodide | HCID 21502450 | — |
| 촉매 | Silver Chloride | HCID 24561 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | [1-Methyl-3-(2,6,6-trimethyl-2-cyclohexenyl)-2(trans)-propenyl]dimethyl(4-chlorobenzyl)ammonium chloride | HCID 21502481 | 111.5% |
반응 단계
A mixture of [1-methyl-3-(2,6,6-trimethyl-2-cyclohexenyl)-2(trans)-propenyl]dimethyl(4-chlorobenzyl)ammonium iodide (2.0 g), silver chloride (1.0 g) and absolute methanol (50 cc) was refluxed for 2 hours, and the reaction mixture was filtered. The solvent of the filtrate was distilled off to give hygroscopic colorless crystals (0.9 g) of [1-methyl-3-(2,6,6-trimethyl-2-cyclohexenyl)-2(trans)-propenyl]dimethyl(4-chlorobenzyl)ammonium chloride.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03988373 |
| 출처 데이터셋 | uspto-grants-1976_10 |
| ORD ID | ord-ab552f525aed427d99a40a348038bef3 |
| 출처 메모 | uspto-grants-1976_10 |