Methyl iodide → 131988-12-0

HRID 1289641노트

반응식

HRID 1289641 반응식
[CH3:1][I:2].[CH2:3]([O:5][C:6]1[C:10]([C:11]2[CH:12]=[N:13][CH:14]=[CH:15][CH:16]=2)=[N:9][S:8][N:7]=1)[CH3:4]>CC(C)=O>[I-:2].[CH2:3]([O:5][C:6]1[C:10]([C:11]2[CH:12]=[N+:13]([CH3:1])[CH:14]=[CH:15][CH:16]=2)=[N:9][S:8][N:7]=1)[CH3:4]

참가 물질

4

반응물 2

HCID 6328Methyl iodideHCID 15180131Pyridine, 3-(4-ethoxy-1,2,5-thiadiazol-3-yl)- (9CI)

생성물 1

HCID 15819042131988-12-0

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

A mixture of methyl iodide (0.3 ml, 5 mmol) and 3-(3-ethoxy-1,2,5-thiadiazol-4-yl)pyridine (520 mg, 2.5 mmol) in acetone (10 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.72 g (83%).

후처리

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 0.72 g (83%)

출처 및 근거

ORD 기록
ord-407b6f6a67d1475eb9d2fe99d50eb007
출처 데이터셋
uspto-grants-1998_05
특허 번호
US05750541

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