Methyl iodide → 3-(3-(3-Methyl-2-butenyloxy)-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide
반응식
[CH3:1][I:2].[CH3:3][C:4]([CH3:19])=[CH:5][CH2:6][O:7][C:8]1[C:12]([C:13]2[CH:14]=[N:15][CH:16]=[CH:17][CH:18]=2)=[N:11][S:10][N:9]=1>CC(C)=O>[I-:2].[CH3:3][C:4]([CH3:19])=[CH:5][CH2:6][O:7][C:8]1[C:12]([C:13]2[CH:14]=[N+:15]([CH3:1])[CH:16]=[CH:17][CH:18]=2)=[N:11][S:10][N:9]=1참가 물질
4
실험 절차
A mixture of methyl iodide (1 ml, 15 mmol) and 3-(3-(3-methyl-2-butenyloxy)-1,2,5-thiadiazol-4-yl)pyridine (3 mmol) in acetone (3 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.92 g (79%).
후처리
- customThe title compound precipitated from the solution
- filtrationwas collected by filtration
- customto yield 0.92 g (79%)
출처 및 근거
- ORD 기록
- ord-210b0c56410f41fa8b68c7de8f2c8d81
- 출처 데이터셋
- uspto-grants-1998_05
- 특허 번호
- US05750541
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