1,2-Dichloroethane → Methyl 3-(4-chlorophenyl)-2-propenoate
반응식
[Cl:1][C:2]1[CH:12]=[CH:11][C:5]([CH:6]=[CH:7][C:8]([OH:10])=[O:9])=[CH:4][CH:3]=1.Cl[CH2:14]CCl.S(=O)(=O)(O)O>CO>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([CH:6]=[CH:7][C:8]([O:10][CH3:14])=[O:9])=[CH:11][CH:12]=1참가 물질
5
실험 절차
The synthesis method of Example 7-(1) was applied. 4-Chlorocinnamic acid (10.0 g), 1,2-dichloroethane (50 methanol (9.0 ml) and concentrated sulfuric acid (0.4 ml) were used as reagents to give 10.2 g of a white solid (yield 95%).
출처 및 근거
- ORD 기록
- ord-0677265866c244d1aee9377bcdf37155
- 출처 데이터셋
- uspto-grants-1998_05
- 특허 번호
- US05750545
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