1,4-Bis(3-aminopropyl)piperazine → N,N'-bis{[N-(2,3,4,5-tetramethoxy-6-methylbenzyl)]-3-aminopropyl}piperazine

HRID 1292017

반응식

HRID 1292017 반응식
[NH2:1][CH2:2][CH2:3][CH2:4][N:5]1[CH2:10][CH2:9][N:8]([CH2:11][CH2:12][CH2:13][NH2:14])[CH2:7][CH2:6]1.[CH3:15][O:16][C:17]1[C:24]([O:25][CH3:26])=[C:23]([O:27][CH3:28])[C:22]([O:29][CH3:30])=[C:21]([CH3:31])[C:18]=1[CH:19]=O>>[CH3:15][O:16][C:17]1[C:24]([O:25][CH3:26])=[C:23]([O:27][CH3:28])[C:22]([O:29][CH3:30])=[C:21]([CH3:31])[C:18]=1[CH2:19][NH:14][CH2:13][CH2:12][CH2:11][N:8]1[CH2:7][CH2:6][N:5]([CH2:4][CH2:3][CH2:2][NH:1][CH2:19][C:18]2[C:21]([CH3:31])=[C:22]([O:29][CH3:30])[C:23]([O:27][CH3:28])=[C:24]([O:25][CH3:26])[C:17]=2[O:16][CH3:15])[CH2:10][CH2:9]1

참가 물질

3

반응물 2

HCID 816291,4-Bis(3-aminopropyl)piperazineHCID 148523342,3,4,5-Tetramethoxy-6-methylbenzaldehyde

생성물 1

HCID 86752610N,N'-bis{[N-(2,3,4,5-tetramethoxy-6-methylbenzyl)]-3-aminopropyl}piperazine

실험 절차

The title compound was prepared by a similar way as in Preparation Example 1, except that 1,4-bis(3-aminopropyl)piperazine was used instead of trans-1,2-cyclohexane diamine and 2,3,4,5-tetramethoxy-6-methylbenzaldehyde was used instead of veratraldehyde.

출처 및 근거

ORD 기록
ord-014d74135f9642098bfd0aedb3bac0db
출처 데이터셋
uspto-grants-1998_05
특허 번호
US05756475

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