Dimethyl Sulfoxide → HCID 86598999, 화합물

HRID 1292975노트

반응식

HRID 1292975 반응식
[CH:1]1([C:6]([OH:19])([CH2:9][C:10]([CH3:18])([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)[CH3:11])[CH2:7][OH:8])[CH2:5][CH2:4][CH2:3][CH2:2]1.CS(C)=O>C(N(CC)CC)C>[CH:1]1([C:6]([OH:19])([CH2:9][C:10]([CH3:11])([C:12]2[CH:13]=[CH:14][CH:15]=[CH:16][CH:17]=2)[CH3:18])[CH:7]=[O:8])[CH2:2][CH2:3][CH2:4][CH2:5]1

참가 물질

4

반응물 2

HCID 679Dimethyl SulfoxideHCID 694236952-Cyclopentyl-4-methyl-4-phenylpentane-1,2-diol

생성물 1

HCID 86598999HCID 86598999, 화합물

시약·촉매·용매 1

HCID 8471Triethylamine용매

실험 절차

185 mg of 2-cyclopentyl-4-methyl-4-phenyl-1,2-pentanediol is converted with 438 mg of pyridine-sulfur trioxide complex, 2.5 ml of DMSO and 0.5 ml of triethylamine into 160 mg of aldehyde.

출처 및 근거

ORD 기록
ord-3e48b72266ce4a549fba70829307b111
출처 데이터셋
uspto-grants-2007_07
특허 번호
US07238707B2

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