Butanal → 56249-61-7

HRID 1295424노트

반응식

HRID 1295424 반응식
[CH:1](=O)[CH2:2][CH2:3][CH3:4].[CH2:6]([NH2:13])[C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1>C1(C)C=CC=CC=1>[CH:1](=[N:13][CH2:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1)[CH2:2][CH2:3][CH3:4]

참가 물질

4

반응물 2

HCID 261ButanalHCID 7504Benzylamine

생성물 1

HCID 455591156249-61-7

시약·촉매·용매 1

HCID 1140Toluene용매

실험 절차

This material is a known compound prepared in the standard fashion. To about 100 mL of toluene was added 28 mL of butyraldehyde, 34 mL of benzylamine, and several grams of 3A molecular sieves. The mixture became warm and turbid after standing for a few minutes. After standing for several hours the mixture was colorless and transparent. The imine product was isolated by distillation under vacuum and characterized by NMR spectroscopy.

후처리

  1. customprepared in the standard fashion
  2. temperatureThe mixture became warm
  3. waitafter standing for a few minutes
  4. waitAfter standing for several hours

출처 및 근거

ORD 기록
ord-975dd027af1d4246842a1aa172023b42
출처 데이터셋
uspto-grants-2007_07
특허 번호
US07241839B2

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