Benzoylacetone → 2-Methyl-1-phenylbutane-1,3-dione

반응식

[C:1]([CH2:9][C:10](=[O:17])[C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)(=[O:8])[C:2]1C=CC=CC=1.[C:18]1(C(=O)CC(=O)C)C=CC=CC=1>>[C:11]1([C:10](=[O:17])[CH:9]([CH3:18])[C:1](=[O:8])[CH3:2])[CH:12]=[CH:13][CH:14]=[CH:15][CH:16]=1

참가 물질

반응물 2

HCID 7166Benzoylacetone

HCID 8433Dibenzoylmethane

생성물 1

HCID 5693692-Methyl-1-phenylbutane-1,3-dione

실험 절차

Synthetic procedure was identical with that described in synthetic example 42(1), except that raw material dibenzoyl methane was replaced by 1-phenyl-1,3-butandione.

출처 및 근거

ORD 기록: ord-721a9390796545f0b4314d4434635ff6
출처 데이터셋: uspto-grants-2008_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07388061B2

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