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[F:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][C:9]2[CH:16]=[CH:15][C:14]([CH:17]([CH3:19])[CH3:18])=[CH:13][C:10]=2[C:11]#[N:12])=[C:4]([N+:20]([O-])=O)[CH:3]=1.[Sn](Cl)[Cl:24]>>[ClH:24].[F:1][C:2]1[CH:7]=[CH:6][C:5]2[NH:8][C:9]3[CH:16]=[CH:15][C:14]([CH:17]([CH3:19])[CH3:18])=[CH:13][C:10]=3[C:11]([NH2:12])=[N:20][C:4]=2[CH:3]=1참가 물질
3
실험 절차
By using a method similar to the method of Example 532, using 2-(4-fluoro-2-nitro-phenylamino)-5-isopropyl-benzonitrile (0.559 g, (1.87 mmol), tin (II) chloride(1.06 g, 5.60 mmol) to obtain (0.422 g, 1.38 mmol, 74% yield) of the title compound as a yellow amorphous solid: Mass Spectrum (m/e): 270(M+1).
출처 및 근거
- ORD 기록
- ord-0a532a107aca4269839c1a5ec59956f2
- 출처 데이터셋
- uspto-grants-2007_05
- 특허 번호
- US07214673B2
연결된 노트
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