2-Methoxyethanol → 2-Methoxyethyl 5-amino-4-oxopentanoate--hydrogen chloride (1/1)

HRID 1351432노트

반응식

HRID 1351432 반응식
[CH3:1][O:2][CH2:3][CH2:4]O.[ClH:6].[NH2:7][CH2:8][C:9](=[O:15])[CH2:10][CH2:11][C:12]([OH:14])=[O:13]>>[ClH:6].[NH2:7][CH2:8][C:9](=[O:15])[CH2:10][CH2:11][C:12]([O:14][CH2:4][CH2:3][O:2][CH3:1])=[O:13]

참가 물질

3

반응물 2

HCID 80192-MethoxyethanolHCID 123608Aminolevulinic Acid Hydrochloride

생성물 1

HCID 426018902-Methoxyethyl 5-amino-4-oxopentanoate--hydrogen chloride (1/1)

실험 절차

From 2-methoxyethanol (5.0 g; 66 mmol) and 5-amino-4-oxopentanoic acid hydrochloride (1.0 g; 6.0 mmol) at 70° C. The reaction was complete after 1 h. The yield was 1.25 g (93%) of yellowish oil.

후처리

  1. customat 70° C

출처 및 근거

ORD 기록
ord-ef889e94cceb41c69864fdb4ab7c0629
출처 데이터셋
uspto-grants-2007_05
특허 번호
US07217736B2

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