Anthranilamide → 2-(Phenylamino)Benzamide

HRID 1354969

반응식

HRID 1354969 반응식
Br[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[NH2:8][C:9]1[CH:17]=[CH:16][CH:15]=[CH:14][C:10]=1[C:11]([NH2:13])=[O:12].CCCCCC>C(OCC)(=O)C>[C:2]1([NH:8][C:9]2[CH:17]=[CH:16][CH:15]=[CH:14][C:10]=2[C:11]([NH2:13])=[O:12])[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

참가 물질

5

반응물 3

HCID 6942AnthranilamideHCID 7961BromobenzeneHCID 8058Hexane

생성물 1

HCID 964552-(Phenylamino)Benzamide수율 70%

시약·촉매·용매 1

HCID 8857Ethyl Acetate용매

실험 절차

Following the general procedure, bromobenzene (55 μL, 0.5 mmol) was coupled with 2-aminobenzamide (102 mg, 0.75 mmol) with the reaction time of 15 h. Chromatography on silica gel column with 1:1 hexane:ethyl acetate gave 74 mg (70%) of the title compound as a white solid.

출처 및 근거

ORD 기록
ord-ac9ec18186204be989636781b1292e6e
출처 데이터셋
uspto-grants-2007_05
특허 번호
US07223879B2

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