Ethylene carbonate → HCID 18186793, 화합물
반응식
[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:10](=[CH:11][CH:12]=1)[CH:9]=[C:8]([OH:13])[CH:7]=[CH:6]2.C1(=O)O[CH2:17][CH2:16][O:15]1>CO.C(Cl)(Cl)Cl.CCCCCC>[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:10](=[CH:11][CH:12]=1)[CH:9]=[C:8]([O:13][CH2:17][CH2:16][OH:15])[CH:7]=[CH:6]2참가 물질
4
실험 절차
*Prepared from 6-methoxy-2-naphthol and ethylene carbonat according to the procedure of Example 134, step 1, in WO 00/76984. The reaction mixture was refluxed for 2 h. Pure 2-(6-methoxy-naphthalen-2-yloxy)ethanol was obtained by recrystallization from MeOH/CHCl3/n-hexane.
후처리
- temperatureThe reaction mixture was refluxed for 2 h
출처 및 근거
- ORD 기록
- ord-414f885c9df546a7866e1c4dbb3a2be7
- 출처 데이터셋
- uspto-grants-2003_07
- 특허 번호
- US06593330B2
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