Potassium Carbonate → HCID 178515855, 화합물
반응식
[CH2:1]([C:8]1[C:13]([Br:14])=[CH:12][N:11]=[C:10]([O:15]C)[CH:9]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.C(=O)([O-])[O-].[K+].[K+]>Br>[CH2:1]([C:8]1[C:13]([Br:14])=[CH:12][N:11]=[C:10]([OH:15])[CH:9]=1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1참가 물질
4
실험 절차
250 ml of 47% hydrobromic acid was added to 62 g of 4-benzyl-5-bromo-2-methoxypyridine, followed by heating under stirring for 3 hours in an oil bath kept at 100° C. After cooling as it was, the reaction solution was added to an aqueous potassium carbonate solution little by little and neutralized. The resulting precipitates were collected by filtration, to give 59 g of the target compound.
후처리
- temperatureby heating
- customkept at 100° C
- temperatureAfter cooling as it
- customThe resulting precipitates
- filtrationwere collected by filtration
출처 및 근거
- ORD 기록
- ord-8c821cdfdc234599beec1c2f718899b5
- 출처 데이터셋
- uspto-grants-2003_07
- 특허 번호
- US06599917B1
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