Isopropylamine → 2-Amino-N-isopropylbenzamide
반응식
[C:1]12[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=1)[NH:6]C(=O)[O:4][C:2]2=O.[CH:13]([NH2:16])([CH3:15])[CH3:14]>O>[NH2:6][C:7]1[CH:8]=[CH:9][CH:10]=[CH:11][C:1]=1[C:2]([NH:16][CH:13]([CH3:15])[CH3:14])=[O:4]참가 물질
4
실험 절차
A round-bottomed flask was charged with isatoic anhydride (5.0 g, 0.030 mol) and 30 mL water. Isopropylamine (4.64 mL, 0.049 mol) was added slowly to the reaction mixture. The product precipitated from the reaction mixture. After 1 h, the reaction mixture was filtered and washed with water to give 4.12 g (71% yield) of a white solid
후처리
- customThe product precipitated from the reaction mixture
- filtrationthe reaction mixture was filtered
- washwashed with water
출처 및 근거
- ORD 기록
- ord-7fc24b27a8664e549d66df96405fa8cf
- 출처 데이터셋
- uspto-grants-2011_02
- 특허 번호
- US07884098B2
반응 노트
불러오는 중…