HCID 70026837, 화합물 → HCID 69959678, 화합물
반응식
[CH3:1][O:2][C:3]1[CH:12]=[C:11]2[C:6]([CH:7]=[CH:8][CH:9]=[C:10]2[CH:13]=[CH:14][C:15]([O:17]CC)=[O:16])=[CH:5][CH:4]=1>C(O)C.[OH-].[Na+]>[CH3:1][O:2][C:3]1[CH:12]=[C:11]2[C:6]([CH:7]=[CH:8][CH:9]=[C:10]2[CH:13]=[CH:14][C:15]([OH:17])=[O:16])=[CH:5][CH:4]=1참가 물질
4
실험 절차
8.4 g (32.8 mmol) of the ester obtained in Step D dissolved in 150 ml of ethanol in the presence of 40 ml of 2N sodium hydroxide solution are stirred for 3 hours at room temperature and overnight at reflux to yield the title acid in the form of a white solid.
후처리
- temperatureat reflux
출처 및 근거
- ORD 기록
- ord-d868500446ce46cc9f297e91d43f37f4
- 출처 데이터셋
- uspto-grants-2003_06
- 특허 번호
- US06583319B1
반응 노트
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