2-Methyl-3-nitroaniline → N-(4-(3-(allyloxy)phenoxy)benzyl)-2-methyl-3-nitroaniline

HRID 1370832노트

반응식

HRID 1370832 반응식
[CH2:1]([O:4][C:5]1[CH:6]=[C:7]([CH:17]=[CH:18][CH:19]=1)[O:8][C:9]1[CH:16]=[CH:15][C:12]([CH:13]=O)=[CH:11][CH:10]=1)[CH:2]=[CH2:3].[CH3:20][C:21]1[C:27]([N+:28]([O-:30])=[O:29])=[CH:26][CH:25]=[CH:24][C:22]=1[NH2:23]>>[CH2:1]([O:4][C:5]1[CH:6]=[C:7]([CH:17]=[CH:18][CH:19]=1)[O:8][C:9]1[CH:16]=[CH:15][C:12]([CH2:13][NH:23][C:22]2[CH:24]=[CH:25][CH:26]=[C:27]([N+:28]([O-:30])=[O:29])[C:21]=2[CH3:20])=[CH:11][CH:10]=1)[CH:2]=[CH2:3]

참가 물질

3

반응물 2

HCID 117832-Methyl-3-nitroanilineHCID 185123024-[3-(Allyloxy)phenoxy]benzaldehyde

생성물 1

HCID 18512125N-(4-(3-(allyloxy)phenoxy)benzyl)-2-methyl-3-nitroaniline수율 82%

실험 절차

The product from Example 61C and 2-methyl-3-nitroaniline were processed as described in Example 6A to provide the title compound (7.20 g, 82%).

출처 및 근거

ORD 기록
ord-bf5533edd7e84a29aba169442e48f929
출처 데이터셋
uspto-grants-2003_06
특허 번호
US06583180B2

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