Hydrochloric Acid → 3-(Ethanesulfonyl)propan-1-amine hydrochloride

HRID 1371399노트

반응식

HRID 1371399 반응식
[CH2:1]([S:3]([CH2:6][CH2:7][CH2:8][NH:9]C(=O)OC(C)(C)C)(=[O:5])=[O:4])[CH3:2].[ClH:17]>O1CCOCC1>[ClH:17].[CH2:1]([S:3]([CH2:6][CH2:7][CH2:8][NH2:9])(=[O:5])=[O:4])[CH3:2]

참가 물질

4

반응물 2

HCID 313Hydrochloric AcidHCID 23089203tert-Butyl 3-(ethylsulfonyl)propylcarbamate

생성물 1

HCID 230892043-(Ethanesulfonyl)propan-1-amine hydrochloride

시약·촉매·용매 1

HCID 312751,4-Dioxane용매

실험 절차

Intermediate 39 (0.275 g) was dissolved in 4M hydrogen chloride in dioxane (3 ml), and the solution was allowed to stand at 22° C. for 2 h. The solvent was evaporated in vacuo to give the title compound as a white solid (186 mg).

후처리

  1. customThe solvent was evaporated in vacuo

출처 및 근거

ORD 기록
ord-d288090551eb491dabb37bae96dc05ac
출처 데이터셋
uspto-grants-2007_01
특허 번호
US07157457B2

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