Water → Actarit

HRID 1375084

반응식

HRID 1375084 반응식
[NH2:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][C:9]([OH:11])=[O:10])=[CH:4][CH:3]=1.[C:12](OC(=O)C)(=[O:14])[CH3:13].O>C(O)(=O)C>[C:12]([NH:1][C:2]1[CH:3]=[CH:4][C:5]([CH2:8][C:9]([OH:11])=[O:10])=[CH:6][CH:7]=1)(=[O:14])[CH3:13]

참가 물질

5

반응물 3

HCID 962WaterHCID 7918Acetic AnhydrideHCID 145334-Aminophenylacetic acid

생성물 1

HCID 2018Actarit

시약·촉매·용매 1

HCID 176Acetic Acid용매

실험 절차

A mixture of (4-amino-phenyl)-acetic acid (25 g) in acetic acid (200 mL) was treated with acetic anhydride (31.3 mL). The mixture was heated on a steam bath for 4 hours, then cooled, then treated with water (20 mL) and then evaporated. The residue was dried under vacuum to give the title compound (30.4 g) as a beige coloured solid.

후처리

  1. temperatureThe mixture was heated on a steam bath for 4 hours
  2. temperaturecooled
  3. customevaporated
  4. customThe residue was dried under vacuum

출처 및 근거

ORD 기록
ord-fbc6011db07f4599837d3cc911c5dfb4
출처 데이터셋
uspto-grants-2007_01
특허 번호
US07166616B2

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