Bromide ion → HCID 13187365, 화합물

HRID 1379971노트

반응식

HRID 1379971 반응식
Cl[CH2:2][C:3]([C:5]1[CH:10]=[CH:9][C:8]([N+:11]([O-:13])=[O:12])=[CH:7][CH:6]=1)=[CH2:4].[F-:14].[K+].[Br-]>O>[F:14][CH2:2][C:3]([C:5]1[CH:10]=[CH:9][C:8]([N+:11]([O-:13])=[O:12])=[CH:7][CH:6]=1)=[CH2:4]

참가 물질

5

반응물 3

HCID 259Bromide ionHCID 522689Potassium FluorideHCID 13187346HCID 13187346, 화합물

생성물 1

HCID 13187365HCID 13187365, 화합물

시약·촉매·용매 1

HCID 962Water용매

실험 절차

Under a N2 blanket is stirred a mixture of 296.5 g (1.5 Mol) 4(1-chloromethyl-ethenyl)-nitrobenzene, 430 g (7.4 Mol) KF, 78 g (0.15 Mol) hexadecyltributylphosphonimine bromide and 800 ml H2O, during 5 hours at 110°-112°.

출처 및 근거

ORD 기록
ord-0de37c3abbb04374a60a8bb586bbd101
출처 데이터셋
uspto-grants-1986_04
특허 번호
US04579585

반응 노트

불러오는 중…