HCID 3335773, 화합물 → 2,3,5,6-Tetraaminocyclohexa-2,5-diene-1,4-dione

HRID 1380283노트

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HRID 1380283 반응식
C1(=O)[N:5]([C:6]2[C:11](=[O:12])[C:10]([N:13]3C(=O)C4=CC=CC=C4C3=O)=[C:9]([N:24]3C(=O)C4=CC=CC=C4C3=O)[C:8](=[O:35])[C:7]=2[N:36]2C(=O)C3=CC=CC=C3C2=O)C(=O)C2=CC=CC=C12>O.NN>[NH2:36][C:7]1[C:8](=[O:35])[C:9]([NH2:24])=[C:10]([NH2:13])[C:11](=[O:12])[C:6]=1[NH2:5]

참가 물질

3

반응물 1

HCID 3335773HCID 3335773, 화합물

생성물 1

HCID 127792772,3,5,6-Tetraaminocyclohexa-2,5-diene-1,4-dione

시약·촉매·용매 1

HCID 24654Hydrazine hydrate (1:1)용매

반응 조건

온도
60 °C

실험 절차

Tetraphthalimido-1,4-benzoquinone (30.00 g, 0.044 mole) is added to 200 ml of 80% hydrazine hydrate. The mixture is heated to 60° C. for two hours. After cooling to room temperature, the mixture is filtered yielding dark purple crystals melting at 260°-262° C.

후처리

  1. temperatureAfter cooling to room temperature
  2. filtrationthe mixture is filtered

출처 및 근거

ORD 기록
ord-79c4bc85ea474ea58c0d970f0468d8de
출처 데이터셋
uspto-grants-1986_04
특허 번호
US04581349

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