HCID 23325188, 화합물 → 4-Aminohex-5-ynoic acid hydrochloride

HRID 1380484노트

반응식

HRID 1380484 반응식
[ClH:1].[NH2:2][CH:3]([C:11]#[CH:12])[CH2:4][CH2:5][C:6]([O:8]CC)=[O:7]>Cl>[ClH:1].[NH2:2][CH:3]([C:11]#[CH:12])[CH2:4][CH2:5][C:6]([OH:8])=[O:7]

참가 물질

3

반응물 1

HCID 23325188HCID 23325188, 화합물

생성물 1

HCID 867407234-Aminohex-5-ynoic acid hydrochloride

시약·촉매·용매 1

HCID 313Hydrochloric Acid용매

실험 절차

A solution of 0.4 g of 1 in 2 ml of concentrated hydrochloric acid was stirred at room temperature for one hour. The water was evaporated. Toluene was added to the residue and distilled to remove residual water by azeotropic distillation. The residue was dried under reduced pressure to give 2, as a hygroscopic solid.

후처리

  1. customThe water was evaporated
  2. additionToluene was added to the residue
  3. distillationdistilled
  4. customto remove residual water
  5. distillationby azeotropic distillation
  6. customThe residue was dried under reduced pressure
  7. customto give 2

출처 및 근거

ORD 기록
ord-120eef4f41cc4363a087d5da0525a238
출처 데이터셋
uspto-grants-1986_04
특허 번호
US04582529

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