Methyl iodide → HCID 19838283, 화합물
반응식
[OH:1][C:2]1[C:3]([CH2:15][CH2:16][CH3:17])=[C:4]([CH:7]=[C:8]([N+:12]([O-:14])=[O:13])[C:9]=1[O:10][CH3:11])[CH:5]=[O:6].[C:18](=O)([O-])[O-].[K+].[K+].CI>CN(C)C=O>[CH3:18][O:1][C:2]1[C:3]([CH2:15][CH2:16][CH3:17])=[C:4]([CH:7]=[C:8]([N+:12]([O-:14])=[O:13])[C:9]=1[O:10][CH3:11])[CH:5]=[O:6]참가 물질
5
실험 절차
A solution of the product from step (c) (40.2 g), potassium carbonate (46.5 g) and methyl iodide (20.9 ml) in dry dimethylformamide (150 ml) was stirred at 20° C. for 16 hours. The solvent was evaporated and the residue quenched with water. The aqueous phase was extracted with ethyl acetate which was washed with brine, dried, filtered and evaporated to leave a yellow oil (27.4 g), MS; m/e 283.
후처리
- customThe solvent was evaporated
- customthe residue quenched with water
- extractionThe aqueous phase was extracted with ethyl acetate which
- washwas washed with brine
- customdried
- filtrationfiltered
- customevaporated
출처 및 근거
- ORD 기록
- ord-8e421a68b100489fbf2b3068782fcb69
- 출처 데이터셋
- uspto-grants-1989_02
- 특허 번호
- US04803225
반응 노트
불러오는 중…