Cyanide → 2-(4-Hydroxyphenyl)-2-methylpropanenitrile

HRID 1382514노트

반응식

HRID 1382514 반응식
[OH:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]([C:11]2C=CC(O)=CC=2)([CH3:10])[CH3:9])=[CH:4][CH:3]=1.[C-]#[N:19]>>[C:11]([C:8]([C:5]1[CH:6]=[CH:7][C:2]([OH:1])=[CH:3][CH:4]=1)([CH3:9])[CH3:10])#[N:19]

참가 물질

3

반응물 2

HCID 5975CyanideHCID 6623Bisphenol A

생성물 1

HCID 144190652-(4-Hydroxyphenyl)-2-methylpropanenitrile

실험 절차

A preferred manner of practicing this invention constitutes heating a solventless mixture of Bisphenol A and cyanide ion in a closed vessel to about 185° C. and maintaining that temperature for about 20 hours to produce 4-(1-cyano-1-methylethyl)phenol. Preferred conversions and yields based on Bisphenol A are about 100 percent and 80 percent respectively.

후처리

  1. temperatureconstitutes heating
  2. temperaturemaintaining that temperature for about 20 hours

출처 및 근거

ORD 기록
ord-07bd86a898284e248e77f28b094b6b70
출처 데이터셋
uspto-grants-1989_02
특허 번호
US04806673

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