Hydrogen Bromide → [2-(2-Thienyl)ethylamino](2-chlorophenyl)acetamide hydrobromide
반응식
[S:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH2:6][CH2:7][NH:8][CH:9]([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=1[Cl:19])[C:10]([NH2:12])=[O:11].[BrH:20]>CC(C)=O>[BrH:20].[S:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH2:6][CH2:7][NH:8][CH:9]([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=1[Cl:19])[C:10]([NH2:12])=[O:11]참가 물질
4
실험 절차
14.7 g (0.05 mol) of [2-(2-thienyl)ethylamino](2-chlorophenyl)acetamide, prepared as described in Example 7, is dissolve din 150 ml of acetone. To the solution 4 ml of 60% aqueous hydrogen bromide solution is added and the precipitated white crystals are filtered off, washed with acetone and dried.
후처리
- dissolutionis dissolve
- filtrationthe precipitated white crystals are filtered off
- washwashed with acetone
- customdried
출처 및 근거
- ORD 기록
- ord-3aa938a98c254de18ce0bedfd69008d4
- 출처 데이터셋
- uspto-grants-2001_07
- 특허 번호
- US06258961B1
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