참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Phenylhydrazine | HCID 7516 | — |
| 반응물 | Fumaronitrile | HCID 637930 | — |
| 생성물 | 2-(Phenylhydrazino)succinonitrile | HCID 53865485 | 45% |
반응 단계
A mixture of phenylhydrazine (4.29 g) and fumaronitrile (3.1 g), where the phenylhydrazine served as a solvent, was heated at 75-80° C. for 20 hours. Purification by flash chromatography on silica gel and crystallization from dichloromethane/hexane gave the title compound (3.29 g, 45%), m.p. 97-98° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06258973B1 |
|---|
| 출처 데이터셋 | uspto-grants-2001_07 |
|---|
| ORD ID | ord-f98160595e9245248d25f1cf5d0add2f |
|---|
| 출처 메모 | uspto-grants-2001_07 |
|---|
