Sodium Hydroxide → 2-Chloro-3-phenyl-4-methylsulfonylbenzoic acid

HRID 1386888노트

반응식

HRID 1386888 반응식
[Cl:1][C:2]1[C:11]([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)=[C:10]([S:18]([CH3:21])(=[O:20])=[O:19])[CH:9]=[CH:8][C:3]=1[C:4]([O:6]C)=[O:5].[OH-].[Na+]>CO>[Cl:1][C:2]1[C:11]([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)=[C:10]([S:18]([CH3:21])(=[O:20])=[O:19])[CH:9]=[CH:8][C:3]=1[C:4]([OH:6])=[O:5]

참가 물질

4

반응물 2

HCID 14798Sodium HydroxideHCID 21183183Methyl 2-chloro-4-methylsulfonyl-3-phenyl-benzoate

생성물 1

HCID 211831732-Chloro-3-phenyl-4-methylsulfonylbenzoic acid

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

Methyl 2-chloro-4-methylsulfonyl-3-phenyl-benzoate was hydrolyzed with sodium hydroxide in aqueous methanol solution and recovered using standard methodology to obtain the title compound, a white solid, which was used as an intermediate without further analysis.

후처리

  1. customrecovered

출처 및 근거

ORD 기록
ord-2587005922b549e7bb728af01212f176
출처 데이터셋
uspto-grants-2001_07
특허 번호
US06265606B1

반응 노트

불러오는 중…