Ammonia → HCID 20297955, 화합물

HRID 1389037노트

반응식

HRID 1389037 반응식
[CH2:1]([N:3]([CH2:14][CH3:15])[C:4]1[CH:5]=[C:6]([CH:11]=[CH:12][CH:13]=1)[CH2:7][CH2:8][C:9]#N)[CH3:2].[OH-:16].[Na+].N.[OH2:19]>>[CH2:1]([N:3]([CH2:14][CH3:15])[C:4]1[CH:5]=[C:6]([CH:11]=[CH:12][CH:13]=1)[CH2:7][CH2:8][C:9]([OH:19])=[O:16])[CH3:2]

참가 물질

5

반응물 4

HCID 222Ammonia2회HCID 962WaterHCID 14798Sodium HydroxideHCID 202979473-[3-(Diethylamino)phenyl]propanenitrile

생성물 1

HCID 20297955HCID 20297955, 화합물

실험 절차

A mixture of 60.6 parts of 3-diethylamino-hydrocinnamonitrile, 250 parts by volume of methylated spirits of denatured alcohol, 100 parts of water and 60 parts by volume of a 35° Be solution of sodium hydroxide was heated under reflux until the evolution of ammonia ceased. After the evolution of ammonia had stopped, the mixture was cooled and then neutralized by addition of 19° Be hydrochloric acid. After filtering and drying, 3-diethylamino-hydrocinnamic acid was obtained of the formula:

후처리

  1. temperaturewas heated
  2. temperaturethe mixture was cooled
  3. filtrationAfter filtering
  4. customdrying

출처 및 근거

ORD 기록
ord-5d1d1314b5084b60b98e18400c3fa9de
출처 데이터셋
uspto-grants-1981_01
특허 번호
US04243606

반응 노트

불러오는 중…