Methyl iodide → HCID 20295270, 화합물

HRID 1389754노트

반응식

HRID 1389754 반응식
[C:1]1([S:7][CH2:8][CH2:9][CH2:10][NH:11][CH2:12][CH2:13][CH:14]([C:21]2[CH:26]=[CH:25][C:24]([OH:27])=[CH:23][CH:22]=2)[C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH2:28](N(CC)CC)C.CI>CO>[CH3:28][N:11]([CH2:12][CH2:13][CH:14]([C:21]1[CH:26]=[CH:25][C:24]([OH:27])=[CH:23][CH:22]=1)[C:15]1[CH:16]=[CH:17][CH:18]=[CH:19][CH:20]=1)[CH2:10][CH2:9][CH2:8][S:7][C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

참가 물질

5

반응물 3

HCID 6328Methyl iodideHCID 8471TriethylamineHCID 202952604-(1-Phenyl-3-{[3-(phenylsulfanyl)propyl]amino}propyl)phenol

생성물 1

HCID 20295270HCID 20295270, 화합물

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

To a solution of 0.8 g (0.0021 moles) of N-(3-phenylthiopropyl)-3-p-hydroxyphenyl-3-phenylpropylamine in 20 ml methanol and containing 0.3 ml triethylamine are added gradually 0.13 ml (0.0021 moles) methyl iodide.

출처 및 근거

ORD 기록
ord-92c8ce1a168a45f68b2fd6a6042be799
출처 데이터셋
uspto-grants-1981_01
특허 번호
US04246201

반응 노트

불러오는 중…