Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium hydride → Sodium 4-chloromethyl-2, 6-di-tert-butylphenoxide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium hydride | HCID 24758 | — |
| 반응물 | 2,6-Di-tert-butyl-4-(chloromethyl)phenol | HCID 12378601 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | Sodium 4-chloromethyl-2, 6-di-tert-butylphenoxide | HCID 23699397 | — |
반응 단계
To a stirred suspension of sodium hydride (2 g.) in dry dimethyl formamide (20 ml.) was added dropwise a solution of 4-chloromethyl-2, 6-di-tert-butylphenol (10 g.) in dimethyl formamide (40 ml.) at 25°-30° C. The mixture was stirred for 30 minutes, during which gas evolution ceased, so as to produce a solution of sodium 4-chloromethyl-2, 6-di-tert-butylphenoxide.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04138389 |
| 출처 데이터셋 | uspto-grants-1979_02 |
| ORD ID | ord-ed335a9a33ba478a905286c3c5f80dc1 |
| 출처 메모 | uspto-grants-1979_02 |