huagongshe.com
HRID1390202

反应详情

EQUATION

反应方程式

HRID 1390202 的结构方程式

REACTANTS

反应物

2
结构：[H-].[Na+]
HCID24758

Sodium hydride

HNa

结构：CC(C)(C)c1cc(CCl)cc(C(C)(C)C)c1O
HCID12378601

2,6-Di-tert-butyl-4-(chloromethyl)phenol

C15H23ClO

PRODUCTS

生成物

1
结构：CC(C)(C)c1cc(CCl)cc(C(C)(C)C)c1[O-].[Na+]
HCID23699397

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

2 次

PROCEDURE

实验过程

To a stirred suspension of sodium hydride (2 g.) in dry dimethyl formamide (20 ml.) was added dropwise a solution of 4-chloromethyl-2, 6-di-tert-butylphenol (10 g.) in dimethyl formamide (40 ml.) at 25°-30° C. The mixture was stirred for 30 minutes, during which gas evolution ceased, so as to produce a solution of sodium 4-chloromethyl-2, 6-di-tert-butylphenoxide.