4-Nitrobenzyl chloride → HCID 21331867, 화합물

HRID 1390977

반응식

HRID 1390977 반응식
[N+:1]([C:4]1[CH:11]=[CH:10][C:7]([CH2:8]Cl)=[CH:6][CH:5]=1)([O-:3])=[O:2].Cl.Cl.[C:14]1(C)[CH:19]=[CH:18][CH:17]=[CH:16][C:15]=1[N:20]1[CH2:25][CH2:24][NH:23][CH2:22][CH2:21]1.[CH2:27](N(CC)CC)C>>[C:18]1([CH3:27])[CH:19]=[CH:14][C:15]([N:20]2[CH2:21][CH2:22][N:23]([CH2:8][C:7]3[CH:10]=[CH:11][C:4]([N+:1]([O-:3])=[O:2])=[CH:5][CH:6]=3)[CH2:24][CH2:25]2)=[CH:16][CH:17]=1

참가 물질

4

반응물 3

HCID 74824-Nitrobenzyl chlorideHCID 8471TriethylamineHCID 919641-(o-Tolyl)piperazine dihydrochloride

생성물 1

HCID 21331867HCID 21331867, 화합물

실험 절차

In the manner given in Example 1A, p-nitrobenzyl chloride is reacted with p-tolylpiperazine dihydrochloride in the presence of triethylamine to give 1-(p-tolyl)-4-(p-nitrobenzyl)piperazine.

출처 및 근거

ORD 기록
ord-d090b32e82fd4da68bdc32cb1afa07d2
출처 데이터셋
uspto-grants-1979_02
특허 번호
US04140775

연결된 노트

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