참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | Isopropanol | HCID 3776 | — |
| 반응물 | N-(2,6-Dichlorobenzoyl)-4-nitro-L-phenylalanine | HCID 58018322 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 4-nitro-N-(2,6-dichlorobenzoyl)-L-phenylalanine isopropylester | HCID 58018321 | — |
반응 단계
Isopropanol (130 mL), tetrahydrofuran (50 mL) and sulfuric acid (0.44 mL) were added to 4-nitro-N-(2,6-dichlorobenzoyl)-L-phenylalanine (2.95 g, 7.70 mmol) and stirred at 50° C. for 5 days. After removing the solvent under reduced pressure, the obtained solid material was washed with water and dried to obtain 3.28 g of a white solid material.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07345049B2 |
|---|
| 출처 데이터셋 | uspto-grants-2008_03 |
|---|
| ORD ID | ord-7f0384011cc04bccb8a0f3eda6d020dd |
|---|
| 출처 메모 | uspto-grants-2008_03 |
|---|
