2-Bromopropane → HCID 12505026, 화합물

HRID 1395107

반응식

HRID 1395107 반응식
[N+:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[SH:10])([O-:3])=[O:2].Br[CH:12]([CH3:14])[CH3:13].C(=O)([O-])[O-].[K+].[K+]>CC(C)=O>[CH:12]([S:10][C:5]1[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=1[N+:1]([O-:3])=[O:2])([CH3:14])[CH3:13]

참가 물질

5

반응물 3

HCID 63582-BromopropaneHCID 11430Potassium CarbonateHCID 21002o-Nitrobenzenethiol

생성물 1

HCID 12505026HCID 12505026, 화합물

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

2-Nitrothiophenol, 2-bromopropane, potassium carbonate and acetone were refluxed for several hours. The solvent then was removed by rotary evaporation. The crude product was partitioned between methylene chloride and a 10% sodium carbonate solution. The organic phase was distilled to yield 2-isopropylmercaptonitrobenzene.

후처리

  1. customThe solvent then was removed by rotary evaporation
  2. customThe crude product was partitioned between methylene chloride
  3. distillationThe organic phase was distilled

출처 및 근거

ORD 기록
ord-d6d6d8edf9324ff78a7de0fc55818bb5
출처 데이터셋
uspto-grants-1980_05
특허 번호
US04202821

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