Diazomethane → HCID 54488354, 화합물
반응식
[Cl:1][C:2]1[CH:18]=[CH:17][C:5]([CH2:6][NH:7][C:8]([S:10][CH2:11][CH2:12][CH2:13][C:14]([OH:16])=[O:15])=[S:9])=[CH:4][CH:3]=1.[N+](=[CH2:21])=[N-]>C(OCC)C>[CH3:21][O:15][C:14](=[O:16])[CH2:13][CH2:12][CH2:11][S:10][C:8](=[S:9])[NH:7][CH2:6][C:5]1[CH:17]=[CH:18][C:2]([Cl:1])=[CH:3][CH:4]=1참가 물질
4
실험 절차
1.5 G. of 4-{[(p-chlorobenzyl)thiocarbamoyl]thio}-butyric acid were dissolved in 30 ml. of diethyl ether and treated with an excess of an ethereal diazomethane solution. The resulting solution was evaporated. The residue was recrystallized from cyclohexane, and 1.2 g. of 4-{[(p-chlorobenzyl)thiocarbamoyl]thio}-butyric acid methyl ester having a melting point of 60°-62° C. were obtained.
후처리
- customThe resulting solution was evaporated
- customThe residue was recrystallized from cyclohexane, and 1.2 g
출처 및 근거
- ORD 기록
- ord-eff9508acb444f87b1c47e2088508cdd
- 출처 데이터셋
- uspto-grants-1980_05
- 특허 번호
- US04202832
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