2-Chloroacetophenone → Phenacyl thiocyanate

HRID 1395618노트

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HRID 1395618 반응식
Cl[CH2:2][C:3]([C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1)=[O:4].[C:11]([S-:13])#[N:12].[K+]>C(O)C.O>[S:13]([CH2:2][C:3]([C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1)=[O:4])[C:11]#[N:12]

참가 물질

5

반응물 2

HCID 107572-ChloroacetophenoneHCID 516872Potassium thiocyanate

생성물 1

HCID 219693Phenacyl thiocyanate

시약·촉매·용매 2

HCID 702Ethanol용매HCID 962Water용매

반응 조건

온도
50 °C

실험 절차

150 g of ω-chloroacetophenone are dissolved at 50° C. in 1000 ml of ethanol, followed by the addition of a solution of 102 g of KSCN in 40 ml of water. After stirring for 10 minutes at 50° C., the ω-thiocyano acetophenone formed is precipitated with water.

출처 및 근거

ORD 기록
ord-7b8bd479b84f475ab2cab32ca67c4a53
출처 데이터셋
uspto-grants-1980_05
특허 번호
US04204867

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